CHEM 4416/6416
UM Chemistry/Graduate/Graduate Courses
Molecular Spectroscopy--CHEM 4416/6416This course is recommended for chemistry and related majors seeking more in-depth study of molecular spectroscopy.
Course Description:
Theory of interaction of light with molecules, in depth theory and application of
spectroscopic techniques nuclear magnetic resonance, mass spectrometry, infrared,
and optical (electronic) spectroscopies. Survey of lesser used methods (electron
spin resonance, microwave, Raman, x-ray crystallography, neutron diffraction, Auger,
Mossbauer, ESCA, AFM, electron microscopy: SEM, and TEM.
Three lecture hours per week; 3 credit hours.
Prerequisite:
CHEM 3310 and 3411 with at least C-. Repeat no more than two times.
Textbook and other materials:
- “Spectrometric Identification of Organic Compounds”, Silverstein, Webster, Kiemle 7th Ed.
Course Objectives:
To provide students with a conceptual and practical understanding of the theory of quantized energy transitions and relationship between molecular structure and energy transitions for different regions of the electromagnetic spectrum. To provide students with appropriate in-depth background in spectroscopic methods for continued studies in any of these areas.
Grades:
Assigned problems, two interval exams and Final, 25% each. Student lecture presentations require a satisfactory evaluation for a passing course grade, Grades are expected to be in the range: A > 85 > B > 75 > C > 55 > D
Policies:
- Within certain restrictions, books and journals may be used to help with take-home tests but not the Internet, and assistance may not be sought from other students or faculty.
- Tardiness and unexcused absence from class are unprofessional behaviors which should be avoided, but attendance will not be graded.
- Electronic devices such as cell phones and pagers should be turned off in the classroom.
- Reasonable and appropriate accommodations will be made for students who present a memo from Student Disability Services.
Academic Integrity and Student Conduct:
Expectations for academic integrity and student conduct are described in detail on the website of the Office of Student Judicial and Ethical Affairs(Student Accountability). Please take a look, in particular, at the sections about “Academic Dishonesty,” “Student Code of Conduct and Responsibilities,” and “Disruptive Behaviors.” I will expect students to be aware of these guidelines and to conduct themselves accordingly.
Reasonable and appropriate accommodations will be provided to students with disabilities who present a memo from Student Disability Services (SDS).
updated 16 February 2017
Course Notes
Section 1: Spectroscopy Theory
updated 19 January 2015
updated 5 February 2015
Section 3: Biomolecular Mass Spectrometry
updated 12 February 2015
Biomolecular Mass Spectrometry Problem Set
updated 12 February 2015
Section 4: Infrared Spectroscopy
updated 19 March 2015
Section 5: Proton NMR Spectroscopy
updated 19 March 2015
Section 6: Carbon and 2D NMR Spectroscopy
updated March 12, 2011
Section 7: Electronic Spectroscopy
updated 19 January 2015
Student PowerPoint Files
AFM
Auger
ESR
Microwave
Mössbauer
Neutron Diffraction
SEM/TEM
X-Ray Diffraction
Student Video Files
AFM
ESR1
ESR2
ESR3
ESR4
Microwave
Mössbauer1
Mössbauer1
X-Ray Diffraction
Problems
4416-6416 Assignments
4406 Documents
44-6406 Information and Guidelines
4406 GC-MS procedure and background
4406 molecular formula determination from MS
GC-MS known structure grade scheme
GC-MS unknown structure grade scheme
updated 15 January 2017